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http://acervodigital.unesp.br/handle/11449/40980
- Title:
- Structural evolution of Eu-doped hydroxyapatite nanorods monitored by photoluminescence emission
- Universidade Federal de São Carlos (UFSCar)
- Empresa Brasileira de Pesquisa Agropecuária (EMBRAPA)
- UFG
- Universidade Estadual Paulista (UNESP)
- Universidade de São Paulo (USP)
- 0925-8388
- Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
- Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
- Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
- Financiadora de Estudos e Projetos (FINEP)
- This paper reports the synthesis of Eu-doped hydroxyapatite (HA:Eu) resulting in particles with nanorod diameters from 9 to 26 nm using the microwave hydrothermal method (HTMW). Eu3+ ions were used as a marker in the HA network by basic hydrolysis followed by the HTMW treatment. The crystalline HA:Eu nanorod nature in a short-range order was detected by photoluminescence (PL) measurements from Eu3+ emission into the HA matrix. Thus, was possible to verify that HA crystallization is favored in a short structural order when the HTMW treatment time was increased from 0 to 40 min and that the Eu3+ substitution in the HA lattice is site-selective. (C) 2012 Elsevier B.V. All rights reserved.
- 5-Aug-2012
- Journal of Alloys and Compounds. Lausanne: Elsevier B.V. Sa, v. 531, p. 50-54, 2012.
- 50-54
- Elsevier B.V. Sa
- Hydroxyapatite
- Europium
- Nanoparticles
- Microwave-hydrothermal method
- Photoluminescence
- http://dx.doi.org/10.1016/j.jallcom.2012.02.053
- Acesso restrito
- outro
- http://repositorio.unesp.br/handle/11449/40980
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