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Effect of air-particle abrasion protocols on the biaxial flexural strength, surface characteristics and phase transformation of zirconia after cyclic loading
  • Clinic for Fixed and Removable Prosthodontics and Dental Materials Science
  • Universidade Estadual Paulista (UNESP)
  • Division of Prosthodontics
  • National Institute of Spatial Research
  • 1751-6161
  • 1878-0180
This study evaluated the effect of air-particle abrasion protocols on the biaxial flexural strength, surface characteristics and phase transformation of zirconia after cyclic loading. Disc-shaped zirconia specimens (Ø: 15mm, thickness: 1.2mm) (N=32) were submitted to one of the air-particle abrasion protocols (n=8 per group): (a) 50μm Al2O3 particles, (b) 110μm Al2O3 particles coated with silica (Rocatec Plus), (c) 30μm Al2O3 particles coated with silica (CoJet Sand) for 20s at 2.8bar pressure. Control group received no air-abrasion. All specimens were initially cyclic loaded (×20,000, 50N, 1Hz) in water at 37°C and then subjected to biaxial flexural strength testing where the conditioned surface was under tension. Zirconia surfaces were characterized and roughness was measured with 3D surface profilometer. Phase transformation from tetragonal to monoclinic was determined by Raman spectroscopy. The relative amount of transformed monoclinic zirconia (FM) and transformed zone depth (TZD) were measured using XRD. The data (MPa) were analyzed using ANOVA, Tukey's tests and Weibull modulus (m) were calculated for each group (95% CI). The biaxial flexural strength (MPa) of CoJet treated group (1266.3±158A) was not significantly different than that of Rocatec Plus group (1179±216.4A,B) but was significantly higher than the other groups (Control: 942.3±74.6C; 50μm Al2O3: 915.2±185.7B,C). Weibull modulus was higher for control (m=13.79) than those of other groups (m=4.95, m=5.64, m=9.13 for group a, b and c, respectively). Surface roughness (Ra) was the highest with 50μm Al2O3 (0.261μm) than those of other groups (0.15-0.195μm). After all air-abrasion protocols, FM increased (15.02%-19.25%) compared to control group (11.12%). TZD also showed increase after air-abrasion protocols (0.83-1.07μm) compared to control group (0.59μm). Air-abrasion protocols increased the roughness and monoclinic phase but in turn abrasion with 30μm Al2O3 particles coated with silica has increased the biaxial flexural strength of the tested zirconia. © 2013 Elsevier Ltd.
Issue Date: 
Journal of the Mechanical Behavior of Biomedical Materials, v. 20, p. 19-28.
Time Duration: 
  • Air-abrasion
  • Biaxial flexural strength
  • Silica coating
  • Y-TZP
  • Zirconia
  • 3D surface
  • Air abrasion
  • Bi-axial flexural strength
  • Control groups
  • Cyclic loadings
  • Monoclinic phase
  • Monoclinic zirconia
  • Rocatec
  • Silica coatings
  • Surface characteristics
  • Weibull modulus
  • XRD
  • Abrasion
  • Aluminum
  • Aluminum coatings
  • Bending strength
  • Cyclic loads
  • Phase transitions
  • Raman spectroscopy
  • Silica
  • Surface roughness
  • Tribology
  • Weibull distribution
  • aluminum oxide
  • silicon dioxide
  • zirconium oxide
  • air particle abrasion protocol
  • biaxial fleural strength
  • controlled study
  • methodology
  • pressure
  • priority journal
  • Raman spectrometry
  • strength
  • X ray diffraction
  • Air
  • Dental Etching
  • Dental Materials
  • Dental Stress Analysis
  • Elastic Modulus
  • Hardness
  • Materials Testing
  • Phase Transition
  • Silicon Dioxide
  • Stress, Mechanical
  • Surface Properties
  • Tensile Strength
  • Zirconium
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Appears in Collections:Artigos, TCCs, Teses e Dissertações da Unesp

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