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- Modeling a system of phosphated cross-linked high amylose for controlled drug release. Part 1: Synthesis and polymer characterization
- Universidade Estadual Paulista (UNESP)
- High amylose was cross-linked with sodium trimetaphosphate (STMP) using 2% and 4% solutions of NaOH at room temperature with reaction contact times of 0.5, 1, 2 and 4 h. The different polymers obtained were analyzed by FT IR, C-13 and P-31 solid state NMR, SEM and C, H and P elemental analysis. The results were used to propose a two-stage mechanism for phosphate incorporation, the first being kinetically controlled. (C) 2008 Elsevier Ltd. All rights reserved.
- Reactive & Functional Polymers. Amsterdam: Elsevier B.V., v. 68, n. 8, p. 1200-1206, 2008.
- Elsevier B.V.
- high amylose
- sodium trimetaphosphate
- reaction kinetics
- Acesso restrito
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