X-ray powder diffraction analysis of a silver(I)-aspartame complex

Putvinskis, R.; Paiva-Santos, C. O.; Cavicchioli, M.; Massabni, Antonio Carlos

Please use this identifier to cite or link to this item: http://acervodigital.unesp.br/handle/11449/38352

Title:

X-ray powder diffraction analysis of a silver(I)-aspartame complex

Author(s):

Institution:

Universidade Estadual Paulista (UNESP)

ISSN:

0885-7156

Abstract:

Synchrotron X-ray powder diffraction (XRPD) data were collected for the silver(I)-aspartame complex [Ag(C14H17N2O5)]center dot 1/2 H2O. The complex was obtained from a stoichiometric mixture of aspartame (3-amino-N-(alpha-carboxyphenethyl)-succinamic acid N-methyl ester, C14H18N2O5), Na2CO3, and AgNO3. Indexing using Crysfire and Chekcell proposed an orthorhombic unit cell with space group P222(1). The lattice parameters are a = 12.4750(1) angstrom, b = 21.60614(14) angstrom, and c = 4.88888(9) angstrom. (C) 2006 International Centre for Diffraction Data.

Issue Date:

1-Dec-2006

Citation:

Powder Diffraction. Newtown Sq: J C P D S-int Centre Diffraction Data, v. 21, n. 4, p. 314-317, 2006.

Time Duration:

314-317

Publisher:

J C P D S-int Centre Diffraction Data

Keywords:

silver(I)-aspartame
X-ray diffraction
Le Bail method

Source:

http://dx.doi.org/10.1154/1.2383065

URI:

Access Rights:

Acesso restrito

Type:

outro

Source:

http://repositorio.unesp.br/handle/11449/38352

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