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Please use this identifier to cite or link to this item: http://acervodigital.unesp.br/handle/11449/25795
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dc.contributor.authorBergamini, Marcio F.-
dc.contributor.authorSantos, Daniela P.-
dc.contributor.authorZanoni, Maria Valnice Boldrin-
dc.date.accessioned2014-05-20T14:19:13Z-
dc.date.accessioned2016-10-25T17:40:57Z-
dc.date.available2014-05-20T14:19:13Z-
dc.date.available2016-10-25T17:40:57Z-
dc.date.issued2010-02-01-
dc.identifierhttp://dx.doi.org/10.1016/j.bioelechem.2009.07.010-
dc.identifier.citationBioelectrochemistry. Lausanne: Elsevier B.V. Sa, v. 77, n. 2, p. 133-138, 2010.-
dc.identifier.issn1567-5394-
dc.identifier.urihttp://hdl.handle.net/11449/25795-
dc.identifier.urihttp://acervodigital.unesp.br/handle/11449/25795-
dc.description.abstractA sensitive voltammetric method for trace measurements of isoniazid (INZ) in synthetic human urine sample is described. The method is based on its electroreduction at -0.98 V vs. Ag/AgCl on screen-printed carbon electrode (SPCE) modified with poly-L-histidine (PH). A film of good adherence on SPCE and electrocatalytic properties was obtained coating the electrode by histidine monomer electropolymerization process (SPCE/EPH). The electrochemical behavior of the modified SPCE was investigated by cyclic, linear sweep (LSV), differential pulse (DPV). square-wave voltammetry (SWV), and electrochemical impedance spectroscopy (EIS). Limits of detection of 5.0 x 10(-7) mol L(-1), 1.7 x 10(-7) mol L(-1) and 2.5 x 10(-7) mol L(-1) were estimated from LSV, DPV and SWV determinations, respectively. The method was successfully applied to the determination of INZ in human urine samples. (c) 2009 Elsevier B.V. All rights reserved.en
dc.description.sponsorshipFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)-
dc.description.sponsorshipCoordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)-
dc.description.sponsorshipConselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)-
dc.format.extent133-138-
dc.language.isoeng-
dc.publisherElsevier B.V. Sa-
dc.sourceWeb of Science-
dc.subjectScreen-printed electrodeen
dc.subjectModified electrodeen
dc.subjectPoly-L-histidineen
dc.subjectIsoniaziden
dc.subjectDeterminationen
dc.titleDetermination of isoniazid in human urine using screen-printed carbon electrode modified with poly-L-histidineen
dc.typeoutro-
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)-
dc.contributor.institutionUniversidade Federal do Paraná (UFPR)-
dc.description.affiliationUNESP, Inst Chem, BR-14801970 Araraquara, SP, Brazil-
dc.description.affiliationUFPR, Ctr Politecn, Dept Quim, Setor Ciencias Exatas, BR-81531990 Curitiba, Parana, Brazil-
dc.description.affiliationUnespUNESP, Inst Chem, BR-14801970 Araraquara, SP, Brazil-
dc.description.sponsorshipIdFAPESP: 03/06598-3-
dc.description.sponsorshipIdFAPESP: 04/00111-8-
dc.identifier.doi10.1016/j.bioelechem.2009.07.010-
dc.identifier.wosWOS:000275232600010-
dc.rights.accessRightsAcesso restrito-
dc.relation.ispartofBioelectrochemistry-
dc.identifier.orcid0000-0002-2296-1393-
Appears in Collections:Artigos, TCCs, Teses e Dissertações da Unesp

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