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Please use this identifier to cite or link to this item: http://acervodigital.unesp.br/handle/11449/25893
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dc.contributor.authorRodrigues, Emanuel C.-
dc.contributor.authorCarvalho, Claudio T.-
dc.contributor.authorde Siqueira, Adriano B.-
dc.contributor.authorBannach, Gilbert-
dc.contributor.authorIonashiro, Massao-
dc.date.accessioned2014-05-20T14:19:31Z-
dc.date.accessioned2016-10-25T17:41:08Z-
dc.date.available2014-05-20T14:19:31Z-
dc.date.available2016-10-25T17:41:08Z-
dc.date.issued2009-12-10-
dc.identifierhttp://dx.doi.org/10.1016/j.tca.2009.07.015-
dc.identifier.citationThermochimica Acta. Amsterdam: Elsevier B.V., v. 496, n. 1-2, p. 156-160, 2009.-
dc.identifier.issn0040-6031-
dc.identifier.urihttp://hdl.handle.net/11449/25893-
dc.identifier.urihttp://acervodigital.unesp.br/handle/11449/25893-
dc.description.abstractSolid-state M-L compounds, where M stands for bivalent Mn, Fe, Co, Ni, Cu, Zn and L is tartrate, have been synthesized. Thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy, elemental analysis and complexometry were used to characterize and to study the thermal behaviour of these compounds. The TG-DTA and DSC curves show that the manganese, cobalt and nickel compounds are hydrated while iron, copper and zinc ones are anhydrous. The thermal stability of the anhydrous compounds depends on the nature of the metal ion, and it follows the order: Zn > Cu > Mn = Co > Ni > Fe. These Curves also show that the thermal decomposition Occurs in a single step to the respective metal oxides. The results led to information about the composition, dehydration, ligand denticity and thermal decomposition of the isolated compounds. (C) 2009 Elsevier B.V. All rights reserved.en
dc.description.sponsorshipUNESP-
dc.description.sponsorshipFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)-
dc.description.sponsorshipConselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)-
dc.description.sponsorshipCoordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)-
dc.format.extent156-160-
dc.language.isoeng-
dc.publisherElsevier B.V.-
dc.sourceWeb of Science-
dc.subjectBivalent metalsen
dc.subjectTartrateen
dc.subjectCharacterizationen
dc.subjectThermal behaviouren
dc.titleSynthesis, characterization and thermal behaviour on solid tartrates of some bivalent metal ionsen
dc.typeoutro-
dc.contributor.institutionCtr Univ Fundação Educ Barretos-
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)-
dc.contributor.institutionUniv Fed Mato Grosso-
dc.contributor.institutionUniversidade de São Paulo (USP)-
dc.description.affiliationCtr Univ Fundação Educ Barretos, BR-14780226 Barretos, SP, Brazil-
dc.description.affiliationUNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil-
dc.description.affiliationUniv Fed Mato Grosso, BR-78698000 Cuiaba, MT, Brazil-
dc.description.affiliationUSP, Inst Quim São Carlos, BR-13560970 São Carlos, SP, Brazil-
dc.description.affiliationUnespUNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil-
dc.identifier.doi10.1016/j.tca.2009.07.015-
dc.identifier.wosWOS:000272853700024-
dc.rights.accessRightsAcesso restrito-
dc.relation.ispartofThermochimica Acta-
Appears in Collections:Artigos, TCCs, Teses e Dissertações da Unesp

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