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Please use this identifier to cite or link to this item: http://acervodigital.unesp.br/handle/11449/26348
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dc.contributor.authorFlumignan, Danilo Luiz-
dc.contributor.authorFerreira, Fabricio de Oliveira-
dc.contributor.authorTininis, Aristeu Gomes-
dc.contributor.authorLopes, Márcia Nasser-
dc.contributor.authorOliveira, Jose Eduardo de-
dc.date.accessioned2014-05-20T14:21:13Z-
dc.date.accessioned2016-10-25T17:41:54Z-
dc.date.available2014-05-20T14:21:13Z-
dc.date.available2016-10-25T17:41:54Z-
dc.date.issued2008-08-22-
dc.identifierhttp://dx.doi.org/10.1016/j.chroma.2008.06.040-
dc.identifier.citationJournal of Chromatography A. Amsterdam: Elsevier B.V., v. 1202, n. 2, p. 181-188, 2008.-
dc.identifier.issn0021-9673-
dc.identifier.urihttp://hdl.handle.net/11449/26348-
dc.identifier.urihttp://acervodigital.unesp.br/handle/11449/26348-
dc.description.abstractThree-step development, optimization and validation strategy for GC fingerprints of Brazilian commercial gasoline is described. A suitable chromatographic system was selected first. The following step was to improve acceptable chromatographic resolution with reduced analysis time, which is recommended for routine applications. Optimization was carried out using full three-level factorial designs. Optimal conditions were obtained for flow rate, oven ramps, injection volume and split ratio. Finally, several validation parameters were performed. Therefore, a feasible and reliable fingerprint was established to identify Brazilian commercial gasoline quality. This strategy can also be applied to develop fingerprints for quality control of other fuels. (C) 2008 Elsevier B.V. All rights reserved.en
dc.description.sponsorshipAgência Nacional do Petróleo, Gás Natural e Biocombustíveis (ANP)-
dc.description.sponsorshipGAS Natural e Biocombustiveis-ANP-
dc.description.sponsorshipFundação para o Desenvolvimento da UNESP (FUNDUNESP)-
dc.description.sponsorshipCoordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)-
dc.description.sponsorshipConselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)-
dc.description.sponsorshipCEMPEQC (Centro de Monitoramento e Pesquisa na Qualidade de Combustiveis, Biocombustiveis, Petroleo e Derivaclos)-
dc.format.extent181-188-
dc.language.isoeng-
dc.publisherElsevier B.V.-
dc.sourceWeb of Science-
dc.subjectgas chromatographic fingerprintingen
dc.subjectmethod developmenten
dc.subjectresponse surface methodologyen
dc.subjectBrazilian commercial gasolineen
dc.subjectquality controlen
dc.titleDevelopment, optimization and validation of gas chromatographic fingerprinting of Brazilian commercial gasoline for quality controlen
dc.typeoutro-
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)-
dc.description.affiliationSão Paulo State Univ UNESP, Inst Chem, Dept Organ Chem, Ctr Monitoring & Res Qual Fuels Biofuels Crude Oi, BR-14800900 Araraquara, SP, Brazil-
dc.description.affiliationUnespSão Paulo State Univ UNESP, Inst Chem, Dept Organ Chem, Ctr Monitoring & Res Qual Fuels Biofuels Crude Oi, BR-14800900 Araraquara, SP, Brazil-
dc.identifier.doi10.1016/j.chroma.2008.06.040-
dc.identifier.wosWOS:000258696800010-
dc.rights.accessRightsAcesso restrito-
dc.relation.ispartofJournal of Chromatography A-
Appears in Collections:Artigos, TCCs, Teses e Dissertações da Unesp

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