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Please use this identifier to cite or link to this item: http://acervodigital.unesp.br/handle/11449/27683
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dc.contributor.authorCarvalho, C. T. de-
dc.contributor.authorSiqueira, A. B.-
dc.contributor.authorIonashiro, E. Y.-
dc.contributor.authorPivatto, M.-
dc.contributor.authorIonashiro, Massao-
dc.date.accessioned2014-05-20T15:10:33Z-
dc.date.accessioned2016-10-25T17:44:57Z-
dc.date.available2014-05-20T15:10:33Z-
dc.date.available2016-10-25T17:44:57Z-
dc.date.issued2008-12-01-
dc.identifierhttp://dx.doi.org/10.1590/S0100-46702008000400008-
dc.identifier.citationEclética Química. Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP, v. 33, n. 4, p. 61-68, 2008.-
dc.identifier.issn0100-4670-
dc.identifier.urihttp://hdl.handle.net/11449/27683-
dc.identifier.urihttp://acervodigital.unesp.br/handle/11449/27683-
dc.description.abstractO ácido 2-metoxicinamalpirúvico (2-MeO-HCP) foi sintetizado e caracterizado por ressonância magnética nuclear (¹H and 13C NMR), espectrometria de massas (MS), espectroscopia na região do infravermelho (FTIR) e calorimetria exploratória diferencial (DSC). A técnica DSC foi usada para determinação da pureza do composto e as principais bandas de absorção na região do infravermelho foram atribuídas utilizando-se o programa GaussView 3.0.pt
dc.description.abstractThe 2-methoxycinnamylidenepyruvic acid (2-MeO-HCP) was synthesized and characterized for nuclear magnetic resonance (¹H and 13C NMR), mass spectrometry (MS), Infrared spectroscopy (FTIR) and differential scanning calorimetry (DSC). The application of DSC for purity determination is well documented in literature and is used in the analysis of pure organic compounds. The molecular geometry and vibrational frequencies of 2-MeO-HCP have been calculated.en
dc.format.extent61-68-
dc.language.isoeng-
dc.publisherEditora Unesp-
dc.sourceSciELO-
dc.subjectácido 2-metoxicinamalpirúvicopt
dc.subjectsíntesept
dc.subjectMSpt
dc.subjectNMRpt
dc.subjectIRpt
dc.subject2-methoxycinnamylidenepyruvic aciden
dc.subjectsynthesisen
dc.subjectMSen
dc.subjectNMRen
dc.subjectIRen
dc.titleSynthesis and characterization of solid 2-methoxycinnamylidenepyruvic aciden
dc.title.alternativeSíntese e caracterização do ácido 2-metoxicinamalpirúvicopt
dc.typeoutro-
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)-
dc.contributor.institutionUFG Instituto de Química-
dc.description.affiliationUNESP Instituto de Química-
dc.description.affiliationUFG Instituto de Química-
dc.description.affiliationUnespUNESP Instituto de Química-
dc.identifier.doi10.1590/S0100-46702008000400008-
dc.identifier.scieloS0100-46702008000400008-
dc.rights.accessRightsAcesso aberto-
dc.identifier.fileS0100-46702008000400008.pdf-
dc.relation.ispartofEclética Química-
Appears in Collections:Artigos, TCCs, Teses e Dissertações da Unesp

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