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dc.contributor.authorLang, E. S.-
dc.contributor.authorLedesma, G. N.-
dc.contributor.authorAbram, U.-
dc.contributor.authorVega-Teijido, M.-
dc.contributor.authorCaracelli, I-
dc.contributor.authorZukerman-Schpector, J.-
dc.date.accessioned2014-05-20T15:25:00Z-
dc.date.accessioned2016-10-25T17:59:19Z-
dc.date.available2014-05-20T15:25:00Z-
dc.date.available2016-10-25T17:59:19Z-
dc.date.issued2006-01-01-
dc.identifierhttp://dx.doi.org/10.1524/zkri.2006.221.2.166-
dc.identifier.citationZeitschrift Fur Kristallographie. Munich: Oldenbourg Verlag, v. 221, n. 2, p. 166-172, 2006.-
dc.identifier.issn0044-2968-
dc.identifier.urihttp://hdl.handle.net/11449/35480-
dc.identifier.urihttp://acervodigital.unesp.br/handle/11449/35480-
dc.description.abstract(1) C11H17IN2STe, Mr = 463.83, P2(1)/n, a 7.6582(8), b = 13.8008(9), c = 15.026(3) angstrom, beta = 96.233(12)degrees, Z = 4, R-1 = 0.0318. (2) C15H19IN2STe, Mr = 513.88, P2(1)/n, a = 8.434(5), b = 11.697(5), c = 18.472(5) angstrom, beta = 98.556(5)degrees, Z = 4, R-1 = 0.0236. The synthesis of the aryltellurenyl N,N',-tetramethylthiourea (tmtu) iodide has been performed by ligand exchange with potassium iodide and the corresponding aryltellurenyl(tmtu) bromide. In both structures the tellurium atom is primarily three-coordinated, being bonded to a carbon atom of the organic ring and, in directions nearly perpendicular to the Te-C bond, to one tmtu sulfur atom and one iodine. In addition there are Te...secondary bonds, joining the molecules in centrosymmetric dimers, which in turn are joined through C-H...1 and C-H... S interactions, in (1) and (2), respectively.en
dc.format.extent166-172-
dc.language.isoeng-
dc.publisherOldenbourg Verlag-
dc.sourceWeb of Science-
dc.subjecttellurium(II)pt
dc.subjecttetramethylthioureapt
dc.subjectsupramolecularpt
dc.subjectX-ray diffractionpt
dc.subjectsingle crystal structure analysispt
dc.titleSynthesis, crystal structure and theoretical studies of aryltellurenyl tetramethylthiourea(tmtu) iodine complexes: Ph-Te(tmtu)I (1) and beta-naphtyl-Te(tmtu)I (2)en
dc.typeoutro-
dc.contributor.institutionUniversidade Federal de Sergipe (UFS)-
dc.contributor.institutionFreien Univ-
dc.contributor.institutionUniversidade Federal de São Carlos (UFSCar)-
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)-
dc.description.affiliationUniversidade Federal de Santa Maria (UFSM), Dept Quim, Lab Mat Inorgan, BR-97105900 Santa Maria, RS, Brazil-
dc.description.affiliationFreien Univ, Inst Chem, Berlin, Germany-
dc.description.affiliationUniv Fed Sao Carlos, Dept Quim, Lab Cristalog Estereodinam & Modelagem Mol, BR-13565905 Sao Carlos, SP, Brazil-
dc.description.affiliationUNESP, Fac Ciências, Bauru, SP, Brazil-
dc.description.affiliationUnespUNESP, Fac Ciências, Bauru, SP, Brazil-
dc.identifier.doi10.1524/zkri.2006.221.2.166-
dc.identifier.wosWOS:000235609900008-
dc.rights.accessRightsAcesso restrito-
dc.relation.ispartofZeitschrift Fur Kristallographie-
Appears in Collections:Artigos, TCCs, Teses e Dissertações da Unesp

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