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http://acervodigital.unesp.br/handle/11449/36584
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DC Field | Value | Language |
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dc.contributor.author | Navickiene, S. | - |
dc.contributor.author | Polese, L. | - |
dc.contributor.author | Minelli, E. V. | - |
dc.contributor.author | Ribeiro, M. L. | - |
dc.date.accessioned | 2014-05-20T15:26:25Z | - |
dc.date.accessioned | 2016-10-25T18:01:02Z | - |
dc.date.available | 2014-05-20T15:26:25Z | - |
dc.date.available | 2016-10-25T18:01:02Z | - |
dc.date.issued | 1999-02-01 | - |
dc.identifier | http://dx.doi.org/10.1007/BF02575288 | - |
dc.identifier.citation | Chromatographia. Wiesbaden: Vieweg, v. 49, n. 3-4, p. 212-214, 1999. | - |
dc.identifier.issn | 0009-5893 | - |
dc.identifier.uri | http://hdl.handle.net/11449/36584 | - |
dc.identifier.uri | http://acervodigital.unesp.br/handle/11449/36584 | - |
dc.description.abstract | A simple and efficient method is described for the determination of fenpropathrin in oranges, pears, apples and strawberries. The procedure: is based on the extraction of each homogenized fruit sample with hexane:acetone (1:1, v/v) mixture, followed, by a cleanup technique on a column packed with florisil, using a hexane:ethyl ether (7:3, v/v) mixture, and gas chromatographic, analysis with electron capture detection (ECD). The fortification levels (0.5; 1.0; 2.0 mg kg(-1)) were selected according to the maximum residue limits (MRLs) established for fenpropathrin by Brazilian legislation. Mean recoveries from five replicates of fortified fruit samples ranged from 83 % to 98 %, with:coefficients of variation from 1.4 to 13.5 and detection limits varying from 0.1 to 0.2 mg kg(-1). | en |
dc.format.extent | 212-214 | - |
dc.language.iso | eng | - |
dc.publisher | Vieweg | - |
dc.source | Web of Science | - |
dc.subject | gas chromatography | pt |
dc.subject | pyrethroid pesticide residues | pt |
dc.subject | fenpropathrin | pt |
dc.subject | fruits | pt |
dc.title | A simplified method for the determination of fenpropathrin residues in fruits | en |
dc.type | outro | - |
dc.contributor.institution | Universidade Estadual Paulista (UNESP) | - |
dc.description.affiliation | UNESP, Inst Quim, Dept Quim Organ, BR-14801970 Araraquara, SP, Brazil | - |
dc.description.affiliationUnesp | UNESP, Inst Quim, Dept Quim Organ, BR-14801970 Araraquara, SP, Brazil | - |
dc.identifier.doi | 10.1007/BF02575288 | - |
dc.identifier.wos | WOS:000078752700017 | - |
dc.rights.accessRights | Acesso restrito | - |
dc.relation.ispartof | Chromatographia | - |
Appears in Collections: | Artigos, TCCs, Teses e Dissertações da Unesp |
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