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Please use this identifier to cite or link to this item: http://acervodigital.unesp.br/handle/11449/36584
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dc.contributor.authorNavickiene, S.-
dc.contributor.authorPolese, L.-
dc.contributor.authorMinelli, E. V.-
dc.contributor.authorRibeiro, M. L.-
dc.date.accessioned2014-05-20T15:26:25Z-
dc.date.accessioned2016-10-25T18:01:02Z-
dc.date.available2014-05-20T15:26:25Z-
dc.date.available2016-10-25T18:01:02Z-
dc.date.issued1999-02-01-
dc.identifierhttp://dx.doi.org/10.1007/BF02575288-
dc.identifier.citationChromatographia. Wiesbaden: Vieweg, v. 49, n. 3-4, p. 212-214, 1999.-
dc.identifier.issn0009-5893-
dc.identifier.urihttp://hdl.handle.net/11449/36584-
dc.identifier.urihttp://acervodigital.unesp.br/handle/11449/36584-
dc.description.abstractA simple and efficient method is described for the determination of fenpropathrin in oranges, pears, apples and strawberries. The procedure: is based on the extraction of each homogenized fruit sample with hexane:acetone (1:1, v/v) mixture, followed, by a cleanup technique on a column packed with florisil, using a hexane:ethyl ether (7:3, v/v) mixture, and gas chromatographic, analysis with electron capture detection (ECD). The fortification levels (0.5; 1.0; 2.0 mg kg(-1)) were selected according to the maximum residue limits (MRLs) established for fenpropathrin by Brazilian legislation. Mean recoveries from five replicates of fortified fruit samples ranged from 83 % to 98 %, with:coefficients of variation from 1.4 to 13.5 and detection limits varying from 0.1 to 0.2 mg kg(-1).en
dc.format.extent212-214-
dc.language.isoeng-
dc.publisherVieweg-
dc.sourceWeb of Science-
dc.subjectgas chromatographypt
dc.subjectpyrethroid pesticide residuespt
dc.subjectfenpropathrinpt
dc.subjectfruitspt
dc.titleA simplified method for the determination of fenpropathrin residues in fruitsen
dc.typeoutro-
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)-
dc.description.affiliationUNESP, Inst Quim, Dept Quim Organ, BR-14801970 Araraquara, SP, Brazil-
dc.description.affiliationUnespUNESP, Inst Quim, Dept Quim Organ, BR-14801970 Araraquara, SP, Brazil-
dc.identifier.doi10.1007/BF02575288-
dc.identifier.wosWOS:000078752700017-
dc.rights.accessRightsAcesso restrito-
dc.relation.ispartofChromatographia-
Appears in Collections:Artigos, TCCs, Teses e Dissertações da Unesp

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