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Please use this identifier to cite or link to this item: http://acervodigital.unesp.br/handle/11449/38531
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dc.contributor.authorTakahashi, P. M.-
dc.contributor.authorFrem, Regina C. G.-
dc.contributor.authorNetto, A. V. G.-
dc.contributor.authorMauro, A. E.-
dc.contributor.authorMatos, J. R.-
dc.date.accessioned2014-05-20T15:28:47Z-
dc.date.accessioned2016-10-25T18:03:58Z-
dc.date.available2014-05-20T15:28:47Z-
dc.date.available2016-10-25T18:03:58Z-
dc.date.issued2007-03-01-
dc.identifierhttp://dx.doi.org/10.1007/s10973-006-7865-y-
dc.identifier.citationJournal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 87, n. 3, p. 797-800, 2007.-
dc.identifier.issn1388-6150-
dc.identifier.urihttp://hdl.handle.net/11449/38531-
dc.identifier.urihttp://acervodigital.unesp.br/handle/11449/38531-
dc.description.abstractThis work describes the synthesis, IR and UV-Vis spectroscopic characterization as well the thermal behavior of the [NiCl2(HIPz)(4)]center dot C3H6O (1), [Ni(H2O)(2)(HIPz)(4)](NO3)(2) (2), [Ni(NCS)(2)(HIPz)(4)] (3) and [Ni(N-3)(2)(HIPz)(4)] (4) (HIPz = 4-iodopyrazole) pyrazolyl complexes. TG experiments reveal that the compounds 1-4 undergo thermal decomposition in three or four mass loss steps yielding NiO as final residue, which was identified by X-ray powder diffraction.en
dc.format.extent797-800-
dc.language.isoeng-
dc.publisherSpringer-
dc.sourceWeb of Science-
dc.subjectDSCpt
dc.subject4-iodopyrazolept
dc.subjectnickel(II)pt
dc.subjectpseudohalidespt
dc.subjectTGpt
dc.titleThermal studies on nickel(II) 4-iodopyrazole complexesen
dc.typeoutro-
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)-
dc.contributor.institutionUniversidade de São Paulo (USP)-
dc.description.affiliationUNESP, Inst Quim Araraquara, BR-14801970 Araraquara, SP, Brazil-
dc.description.affiliationUniv São Paulo, Inst Quim, São Paulo, Brazil-
dc.description.affiliationUnespUNESP, Inst Quim Araraquara, BR-14801970 Araraquara, SP, Brazil-
dc.identifier.doi10.1007/s10973-006-7865-y-
dc.identifier.wosWOS:000244823700037-
dc.rights.accessRightsAcesso restrito-
dc.relation.ispartofJournal of Thermal Analysis and Calorimetry-
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