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Please use this identifier to cite or link to this item: http://acervodigital.unesp.br/handle/11449/39978
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dc.contributor.authorDemarchi, ACCO-
dc.contributor.authorMenezes, Manoel Lima de-
dc.contributor.authorMercadante, A.-
dc.contributor.authorVassillief, I-
dc.date.accessioned2014-05-20T15:30:39Z-
dc.date.accessioned2016-10-25T18:06:13Z-
dc.date.available2014-05-20T15:30:39Z-
dc.date.available2016-10-25T18:06:13Z-
dc.date.issued2001-09-01-
dc.identifierhttp://dx.doi.org/10.1007/BF02492692-
dc.identifier.citationChromatographia. Wiesbaden: Vieweg, v. 54, n. 5-6, p. 402-404, 2001.-
dc.identifier.issn0009-5893-
dc.identifier.urihttp://hdl.handle.net/11449/39978-
dc.identifier.urihttp://acervodigital.unesp.br/handle/11449/39978-
dc.description.abstractSodium monofluoroacetate (NAFAc) has been widely used for vertebrate pest control, such as rabbits in Australia. However NAFAc is extremely toxic to all vertebrates and its use is restricted. Although this compound is stringently restricted, the occurrence of accidental and homicidal poisoning is no ever-present possibility.The method developed in this work shows the applicability of SPE with alumina cartridges for the extraction of NAFAc from serum samples. The method is efficient with recoveries of at least 96.8% from spiked serum. The samples were subsequently derivatized with dicyclohexylcabodiimide (DCC), using 2,4-dichloroaniline (DCA), to make the product volatile for GC analysis.en
dc.format.extent402-404-
dc.language.isoeng-
dc.publisherVieweg-
dc.sourceWeb of Science-
dc.subjectgas chromatographypt
dc.subjectsodium monofluoroacetatept
dc.subjectrodentspt
dc.subjectaluminapt
dc.titleDetermination of the sodium monofluoroacetate in serum by gas chromatographyen
dc.typeoutro-
dc.contributor.institutionUniversidade do Sagrado Coração (USC)-
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)-
dc.description.affiliationUniv Sagrado Coracao, Lab Anal & Pesquisas Clin, BR-17044160 São Paulo, Brazil-
dc.description.affiliationUniv Estadual Paulista, Dept Quim, UNESP, BR-17033360 São Paulo, Brazil-
dc.description.affiliationUniv Estadual Paulista, UNESP, Ctr Atendimento Toxicol, BR-18618000 São Paulo, Brazil-
dc.description.affiliationUnespUniv Estadual Paulista, Dept Quim, UNESP, BR-17033360 São Paulo, Brazil-
dc.description.affiliationUnespUniv Estadual Paulista, UNESP, Ctr Atendimento Toxicol, BR-18618000 São Paulo, Brazil-
dc.identifier.doi10.1007/BF02492692-
dc.identifier.wosWOS:000171316600020-
dc.rights.accessRightsAcesso restrito-
dc.relation.ispartofChromatographia-
Appears in Collections:Artigos, TCCs, Teses e Dissertações da Unesp

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