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DC Field | Value | Language |
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dc.contributor.author | Menezes, Manoel Lima de | - |
dc.contributor.author | Simionato, E. M. R. S. | - |
dc.contributor.author | Felix, G. | - |
dc.date.accessioned | 2014-05-20T15:31:18Z | - |
dc.date.accessioned | 2016-10-25T18:07:04Z | - |
dc.date.available | 2014-05-20T15:31:18Z | - |
dc.date.available | 2016-10-25T18:07:04Z | - |
dc.date.issued | 2008-01-01 | - |
dc.identifier | http://dx.doi.org/10.1080/10826070802352827 | - |
dc.identifier.citation | Journal of Liquid Chromatography & Related Technologies. Philadelphia: Taylor & Francis Inc, v. 31, n. 17, p. 2603-2611, 2008. | - |
dc.identifier.issn | 1082-6076 | - |
dc.identifier.uri | http://hdl.handle.net/11449/40470 | - |
dc.identifier.uri | http://acervodigital.unesp.br/handle/11449/40470 | - |
dc.description.abstract | A new IS-anionic stationary phase was synthesized to make on-line extraction of the ochratoxin A and B from samples of beer for HPLC. The propyltriethylammonium chloride stationary phase was characterized affecting it's elementary determination and RI specter, respectively. Evaluation of the IS-anionic column for the extraction and quantification of OTA and OTB in beer has shown that the column is suitable for efficient extraction (recovery >76.5%) and precise analysis. The detection limits for OTA and OTB were 0.03 and 0.07 mu g L(-1), respectively. The range of detector linearity was 0.03 at 20 mu g L(-1). | en |
dc.description.sponsorship | Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP) | - |
dc.format.extent | 2603-2611 | - |
dc.language.iso | eng | - |
dc.publisher | Taylor & Francis Inc | - |
dc.source | Web of Science | - |
dc.subject | beer | en |
dc.subject | internal surface-anionic | en |
dc.subject | ochratoxin | en |
dc.subject | stationary phase | en |
dc.title | Synthesis of the stationary phase IS-Anionic (internal surface-anionic) for extraction of ochratoxin A and B from samples of beers | en |
dc.type | outro | - |
dc.contributor.institution | Universidade Estadual Paulista (UNESP) | - |
dc.contributor.institution | USC | - |
dc.contributor.institution | Univ Aix Marseille 2 | - |
dc.description.affiliation | Univ Estadual Paulista, Fac Ciencias, Dept Quim, BR-17033360 São Paulo, Brazil | - |
dc.description.affiliation | USC, Lab Alimentos, São Paulo, Brazil | - |
dc.description.affiliation | Univ Aix Marseille 2, Lab Chimie Organ & Mat Mol, CNRS, UMR 6114, Marseille, France | - |
dc.description.affiliationUnesp | Univ Estadual Paulista, Fac Ciencias, Dept Quim, BR-17033360 São Paulo, Brazil | - |
dc.identifier.doi | 10.1080/10826070802352827 | - |
dc.identifier.wos | WOS:000258898600006 | - |
dc.rights.accessRights | Acesso restrito | - |
dc.relation.ispartof | Journal of Liquid Chromatography & Related Technologies | - |
Appears in Collections: | Artigos, TCCs, Teses e Dissertações da Unesp |
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