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http://acervodigital.unesp.br/handle/11449/41217
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DC Field | Value | Language |
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dc.contributor.author | Carvalho, C. T. | - |
dc.contributor.author | Caires, Flavio J. | - |
dc.contributor.author | Lima, L. S. | - |
dc.contributor.author | Ionashiro, Massao | - |
dc.date.accessioned | 2014-05-20T15:32:16Z | - |
dc.date.accessioned | 2016-10-25T18:08:26Z | - |
dc.date.available | 2014-05-20T15:32:16Z | - |
dc.date.available | 2016-10-25T18:08:26Z | - |
dc.date.issued | 2012-03-01 | - |
dc.identifier | http://dx.doi.org/10.1007/s10973-011-1679-2 | - |
dc.identifier.citation | Journal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 107, n. 3, p. 863-868, 2012. | - |
dc.identifier.issn | 1388-6150 | - |
dc.identifier.uri | http://hdl.handle.net/11449/41217 | - |
dc.identifier.uri | http://acervodigital.unesp.br/handle/11449/41217 | - |
dc.description.abstract | Solid-state M-2-MeO-CP compounds, where M represents bivalent Mn, Fe, Co, Ni, Cu, Zn and 2-MeO-CP is 2-methoxycinnamylidenepyruvate, were synthesized for the first time. Simultaneous thermogravimetry and differential thermal analysis, differential scanning calorimetry, X-ray powder diffractometry, infrared spectroscopy, TG-FTIR system, elemental analysis and complexometry have been used to characterize and to study the thermal behaviour of the compounds. The dehydration in all the compounds, except for iron occurs in a single step. The thermal decomposition of the anhydrous compounds occurs in two or three steps with the formation of the respective oxides, Mn3O4, Fe2O3, Co3O4, NiO, CuO and ZnO, as final residue. The results also provided information concerning the thermal behaviour and identification of the gaseous products evolved during the heating of these compounds. | en |
dc.description.sponsorship | Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP) | - |
dc.description.sponsorship | Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq) | - |
dc.description.sponsorship | Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES) | - |
dc.format.extent | 863-868 | - |
dc.language.iso | eng | - |
dc.publisher | Springer | - |
dc.source | Web of Science | - |
dc.subject | Bivalent transition metals | en |
dc.subject | 2-methoxycinnamylidenepyruvate | en |
dc.subject | Thermal behaviour | en |
dc.title | Thermal investigation of solid 2-methoxycinnamylidenepyruvate of some bivalent transition metal ions | en |
dc.type | outro | - |
dc.contributor.institution | Universidade Federal da Grande Dourados (UFGD) | - |
dc.contributor.institution | Universidade Estadual Paulista (UNESP) | - |
dc.description.affiliation | Fundação Univ Fed Grande Dourados, Dourados, MS, Brazil | - |
dc.description.affiliation | UNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil | - |
dc.description.affiliationUnesp | UNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil | - |
dc.identifier.doi | 10.1007/s10973-011-1679-2 | - |
dc.identifier.wos | WOS:000302703400001 | - |
dc.rights.accessRights | Acesso restrito | - |
dc.relation.ispartof | Journal of Thermal Analysis and Calorimetry | - |
Appears in Collections: | Artigos, TCCs, Teses e Dissertações da Unesp |
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