Utilize este identificador para citar ou criar um link para este item:
http://acervodigital.unesp.br/handle/11449/42049
Registro de metadados completo
Campo DC | Valor | Idioma |
---|---|---|
dc.contributor.author | Motta, F. V. | - |
dc.contributor.author | Lima, R. C. | - |
dc.contributor.author | Marques, A. P. A. | - |
dc.contributor.author | Leite, E. R. | - |
dc.contributor.author | Varela, José Arana | - |
dc.contributor.author | Longo, Elson | - |
dc.date.accessioned | 2014-05-20T15:33:26Z | - |
dc.date.accessioned | 2016-10-25T18:09:59Z | - |
dc.date.available | 2014-05-20T15:33:26Z | - |
dc.date.available | 2016-10-25T18:09:59Z | - |
dc.date.issued | 2010-11-01 | - |
dc.identifier | http://dx.doi.org/10.1016/j.materresbull.2010.06.056 | - |
dc.identifier.citation | Materials Research Bulletin. Oxford: Pergamon-Elsevier B.V. Ltd, v. 45, n. 11, p. 1703-1706, 2010. | - |
dc.identifier.issn | 0025-5408 | - |
dc.identifier.uri | http://hdl.handle.net/11449/42049 | - |
dc.identifier.uri | http://acervodigital.unesp.br/handle/11449/42049 | - |
dc.description.abstract | The simple way to prepare In2O3 microcrystals is reported in this paper. The precursor, In(OH)(3) microstructures, were obtained using the Microwave-Assisted Hydrothermal (MAH) Method. By annealing as-prepared In(OH)(3) precursor at 500 degrees C for 5 min in a domestic microwave oven (MO), In2O3 microcrystals were prepared, inheriting the morphology of their precursor while still slightly distorted and collapsed due to the In(OH)(3) dehydration process which was studied by thermal analysis. The In(OH)(3) and In2O3 were characterized using powder X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and Raman spectroscopy. These techniques confirm the chemical dehydration of In(OH)(3) and the formation of In2O3 powders. The domestic MO promotes a rapid structural organization as compared with a CF (conventional furnace). The MAH method and the subsequent annealing in a domestic MO were shown to be a low cost route for the production of In2O3, with the advantages of lower temperature and smaller time. (C) 2010 Elsevier Ltd. All rights reserved. | en |
dc.description.sponsorship | Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP) | - |
dc.description.sponsorship | Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq) | - |
dc.description.sponsorship | Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES) | - |
dc.format.extent | 1703-1706 | - |
dc.language.iso | eng | - |
dc.publisher | Pergamon-Elsevier B.V. Ltd | - |
dc.source | Web of Science | - |
dc.subject | Oxides | en |
dc.subject | Semiconductors | en |
dc.subject | Chemical synthesis | en |
dc.subject | Electron microscopy | en |
dc.title | In2O3 microcrystals obtained from rapid calcination in domestic microwave oven | en |
dc.type | outro | - |
dc.contributor.institution | Universidade Estadual Paulista (UNESP) | - |
dc.contributor.institution | Universidade Federal de Uberlândia (UFU) | - |
dc.contributor.institution | Universidade Federal de São Carlos (UFSCar) | - |
dc.description.affiliation | UNESP, IQ, LIEC, BR-14801907 Araraquara, SP, Brazil | - |
dc.description.affiliation | Universidade Federal de Uberlândia (UFU), IQ, BR-38400902 Uberlandia, MG, Brazil | - |
dc.description.affiliation | Universidade Federal de São Carlos (UFSCar), DQ, LIEC, BR-13565905 São Carlos, SP, Brazil | - |
dc.description.affiliationUnesp | UNESP, IQ, LIEC, BR-14801907 Araraquara, SP, Brazil | - |
dc.description.sponsorshipId | FAPESP: 98/14324-8 | - |
dc.identifier.doi | 10.1016/j.materresbull.2010.06.056 | - |
dc.identifier.wos | WOS:000283907100028 | - |
dc.rights.accessRights | Acesso restrito | - |
dc.relation.ispartof | Materials Research Bulletin | - |
Aparece nas coleções: | Artigos, TCCs, Teses e Dissertações da Unesp |
Não há nenhum arquivo associado com este item.
Itens do Acervo digital da UNESP são protegidos por direitos autorais reservados a menos que seja expresso o contrário.