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Please use this identifier to cite or link to this item: http://acervodigital.unesp.br/handle/11449/65141
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dc.contributor.authorCabras, Paolo-
dc.contributor.authorAngioni, Alberto-
dc.contributor.authorGarau, Vincenzo L.-
dc.contributor.authorMeselli, Elizabeth V.-
dc.date.accessioned2014-05-27T11:18:14Z-
dc.date.accessioned2016-10-25T18:14:31Z-
dc.date.available2014-05-27T11:18:14Z-
dc.date.available2016-10-25T18:14:31Z-
dc.date.issued1997-07-01-
dc.identifierhttp://www.ncbi.nlm.nih.gov/pubmed/9241848-
dc.identifier.citationJournal of AOAC International, v. 80, n. 4, p. 867-870, 1997.-
dc.identifier.issn1060-3271-
dc.identifier.urihttp://hdl.handle.net/11449/65141-
dc.identifier.urihttp://acervodigital.unesp.br/handle/11449/65141-
dc.description.abstractA rapid and simple gas chromatographic method for determinating cyprodinil, fludioxonil, pyrimethanil, and tebuconazole in grapes, must, and wine is described. An on-line microextraction method was used with a one-step extraction-partition procedure. Nitrogen-phosphorus and mass spectrometric detectors were used, because of their low sensitivity and high selectivity. Because of high selectivity of detector, no cleanup was necessary and the extract was concentrated 5 times. Recoveries from fortified grapes, must, and wine ranged from 93 to 110%. Limits of determination were 0.05 mg/kg for cyprodinil and pyrimethanil and 0.10 mg/kg for fludioxonil and tebuconazole.en
dc.format.extent867-870-
dc.language.isoeng-
dc.sourceScopus-
dc.subject1,3 dioxolane derivative-
dc.subjectcyprodinil-
dc.subjectfludioxonil-
dc.subjectfungicide-
dc.subjectnitrogen-
dc.subjectpesticide residue-
dc.subjectphosphorus-
dc.subjectpyrimethanil-
dc.subjectpyrimidine derivative-
dc.subjectpyrrole derivative-
dc.subjecttebuconazole-
dc.subjecttriazole derivative-
dc.subjectchemistry-
dc.subjectfood analysis-
dc.subjectfruit-
dc.subjectgas chromatography-
dc.subjectmass fragmentography-
dc.subjectreproducibility-
dc.subjectstandard-
dc.subjectwine-
dc.subjectChromatography, Gas-
dc.subjectDioxoles-
dc.subjectFood Analysis-
dc.subjectFruit-
dc.subjectFungicides, Industrial-
dc.subjectGas Chromatography-Mass Spectrometry-
dc.subjectNitrogen-
dc.subjectPesticide Residues-
dc.subjectPhosphorus-
dc.subjectPyrimidines-
dc.subjectPyrroles-
dc.subjectReference Standards-
dc.subjectReproducibility of Results-
dc.subjectTriazoles-
dc.subjectWine-
dc.titleGas Chromatographic Determination of Cyprodinil, Fludioxonil, Pyrimethanil, and Tebuconazole in Grapes, Must, and Wineen
dc.typeoutro-
dc.contributor.institutionDipartimento di Tossicologia-
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)-
dc.description.affiliationUniversità di Cagliari Dipartimento di Tossicologia, Viale Diaz 182, 09126 Cagliari-
dc.description.affiliationUniversidade Estadual Paulista Departamento de Quimica Organica, Araraquara, Sao Paulo-
dc.description.affiliationUnespUniversidade Estadual Paulista Departamento de Quimica Organica, Araraquara, Sao Paulo-
dc.identifier.wosWOS:A1997XL99800022-
dc.rights.accessRightsAcesso restrito-
dc.relation.ispartofJournal of AOAC International-
dc.identifier.scopus2-s2.0-0031179761-
Appears in Collections:Artigos, TCCs, Teses e Dissertações da Unesp

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