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Please use this identifier to cite or link to this item: http://acervodigital.unesp.br/handle/11449/66978
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dc.contributor.authorVon Poelhsitz, Gustavo-
dc.contributor.authorDe Araujo, Màrcio Perez-
dc.contributor.authorDe Oliveira, Luiz Antonio Andrade-
dc.contributor.authorQueiroz, Salete Linhares-
dc.contributor.authorEllena, Javier-
dc.contributor.authorCastellano, Eduardo Ernesto-
dc.contributor.authorFerreira, Antonio Gilberto-
dc.contributor.authorBatista, Alzir Azovedo-
dc.date.accessioned2014-05-27T11:20:30Z-
dc.date.accessioned2016-10-25T18:17:58Z-
dc.date.available2014-05-27T11:20:30Z-
dc.date.available2016-10-25T18:17:58Z-
dc.date.issued2002-10-01-
dc.identifierhttp://dx.doi.org/10.1016/S0277-5387(02)01166-X-
dc.identifier.citationPolyhedron, v. 21, n. 22, p. 2221-2225, 2002.-
dc.identifier.issn0277-5387-
dc.identifier.urihttp://hdl.handle.net/11449/66978-
dc.identifier.urihttp://acervodigital.unesp.br/handle/11449/66978-
dc.description.abstractThe fac-[RuCl3(NO)(dppb)] complex I has been prepared from solution of the correspondent mer isomer in refluxing methanol (dppb = 1,4-bis(diphenylphosphino)butane). The mer-[RuCl3(NO)(diop)] (II) has been obtained from the mer-[RuCl3(diop)(H2O)] by bubbling NO for 1 h in dichloromethane (diop = 2S,3S-O-isopropylidene-2,3-dihydroxy-1,4-bis(diphenylphosphino)butane). The complexes have been characterized by microanalysis, cyclic voltammetry (CV), IR and 31P{1H} NMR spectroscopies. The crystal and molecular structures of these two compounds have been determined from X-ray studies. The mer-[RuCl3(NO)(dppb)] isomer III was characterized in solution by NMR spectra (31P{1H}, 1H{31P}, 31P-1H HETCORR, COSY 1H-1H, HMQC 1H-13C and HMBC 1H-13C). © 2002 Elsevier Science Ltd. All rights reserved.en
dc.format.extent2221-2225-
dc.language.isoeng-
dc.sourceScopus-
dc.subjectDiop-
dc.subjectDppb-
dc.subjectNitrosyl complexes-
dc.subjectNMR spectra-
dc.subjectRuthenium(II)-
dc.subjectX-ray structures-
dc.subjectisopropylidene 2,3 dihydroxy 1,4 bis(diphenylphosphino)butane-
dc.subjectmetal complex-
dc.subjectmethanol 1,4 bis(diphenylphosphino)butane-
dc.subjectruthenium complex-
dc.subjectunclassified drug-
dc.subjectanalytic method-
dc.subjectcatalysis-
dc.subjectchemical analysis-
dc.subjectcomplex formation-
dc.subjectnuclear magnetic resonance-
dc.subjectphase transition-
dc.subjectstructure analysis-
dc.subjectsynthesis-
dc.subjectX ray analysis-
dc.titlefac-[RuCl3(no)(dppb)] (I) and mer-[RuCl3(NO)(diop)] (II) complexes: Syntheses, characterization and x-ray structuresen
dc.typeoutro-
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)-
dc.contributor.institutionFaculdade de Ciências de Barretos-
dc.contributor.institutionUniversidade de São Paulo (USP)-
dc.contributor.institutionUniversidade Federal de São Carlos (UFSCar)-
dc.description.affiliationInstituto de Química Universidade Estadual Paulista, C.P. 355, CEP 14800-900 Araraquara, SP-
dc.description.affiliationFaculdade de Ciências de Barretos, Av. Prof. Roberto Frade Monte, 389, CEP 14783-226 Barretos, SP-
dc.description.affiliationInstituto de Física de São Carlos Universidade de São Paulo, C.P. 369, CEP 13560-970 São Carlos, SP-
dc.description.affiliationDepartamento de Química Universidade Federal de São Carlos, C.P. 676, CEP 13565-905 São Carlos, SP-
dc.description.affiliationUnespInstituto de Química Universidade Estadual Paulista, C.P. 355, CEP 14800-900 Araraquara, SP-
dc.identifier.doi10.1016/S0277-5387(02)01166-X-
dc.identifier.wosWOS:000178534400003-
dc.rights.accessRightsAcesso restrito-
dc.relation.ispartofPolyhedron-
dc.identifier.scopus2-s2.0-0036792080-
Appears in Collections:Artigos, TCCs, Teses e Dissertações da Unesp

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