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DC Field | Value | Language |
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dc.contributor.author | Barra, Carolina V. | - |
dc.contributor.author | Rocha, Fillipe V. | - |
dc.contributor.author | Netto, Adelino Vieira de Godoy | - |
dc.contributor.author | Frem, Regina Célia Galvão | - |
dc.contributor.author | Mauro, Antonio Eduardo | - |
dc.contributor.author | Carlos, Iracilda Z. | - |
dc.contributor.author | Ananias, Sandra R. | - |
dc.contributor.author | Quilles, Marcela B. | - |
dc.date.accessioned | 2014-05-20T13:23:56Z | - |
dc.date.accessioned | 2016-10-25T16:44:47Z | - |
dc.date.available | 2014-05-20T13:23:56Z | - |
dc.date.available | 2016-10-25T16:44:47Z | - |
dc.date.issued | 2011-11-01 | - |
dc.identifier | http://dx.doi.org/10.1007/s10973-011-1393-0 | - |
dc.identifier.citation | Journal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 106, n. 2, p. 489-494, 2011. | - |
dc.identifier.issn | 1388-6150 | - |
dc.identifier.uri | http://hdl.handle.net/11449/7312 | - |
dc.identifier.uri | http://acervodigital.unesp.br/handle/11449/7312 | - |
dc.description.abstract | This study describes the synthesis, IR, (1)H, and (13)C{(1)H} NMR spectroscopic as well the thermal characterization of the new palladium(II) pyrazolyl complexes [PdCl(2)(HmPz)(2)] 1, [PdBr(2)(HmPz)(2)] 2, [PdI(2)(HmPz)(2)] 3, [Pd(SCN)(2)(HmPz)(2)] 4 {HmPz = 4-methylpyrazole}. The residues of the thermal decomposition were identified as Pd(0) by X-ray powder diffraction. From the initial decomposition temperatures, the thermal stability of the complexes can be ordered in the sequence: 1 > 2 > 4 a parts per thousand 3. The cytotoxic activities of the complexes and the ligand were investigated against two murine cancer cell lines: mammary adenocarcinoma (LM3) and lung adenocarcinoma (LP07) and compared to cisplatin under the same experimental conditions. | en |
dc.format.extent | 489-494 | - |
dc.language.iso | eng | - |
dc.publisher | Springer | - |
dc.source | Web of Science | - |
dc.subject | DTA | en |
dc.subject | Palladium(II) | en |
dc.subject | Pyrazoles | en |
dc.subject | Spectroscopy | en |
dc.subject | TG | en |
dc.title | New palladium(II) complexes with pyrazole ligands Part II. Synthesis, spectral and thermal studies, and antitumor evaluation | en |
dc.type | outro | - |
dc.contributor.institution | Universidade Estadual Paulista (UNESP) | - |
dc.description.affiliation | UNESP Univ Estadual Paulista, Inst Quim Araraquara, Dept Quim Geral & Inorgan, BR-14801970 Araraquara, SP, Brazil | - |
dc.description.affiliation | UNESP Univ Estadual Paulista, Dept Anal Clin, Fac Ciencias Farmaceut Araraquara, BR-14801902 Araraquara, SP, Brazil | - |
dc.description.affiliationUnesp | UNESP Univ Estadual Paulista, Inst Quim Araraquara, Dept Quim Geral & Inorgan, BR-14801970 Araraquara, SP, Brazil | - |
dc.description.affiliationUnesp | UNESP Univ Estadual Paulista, Dept Anal Clin, Fac Ciencias Farmaceut Araraquara, BR-14801902 Araraquara, SP, Brazil | - |
dc.identifier.doi | 10.1007/s10973-011-1393-0 | - |
dc.identifier.wos | WOS:000296065100029 | - |
dc.rights.accessRights | Acesso restrito | - |
dc.relation.ispartof | Journal of Thermal Analysis and Calorimetry | - |
Appears in Collections: | Artigos, TCCs, Teses e Dissertações da Unesp |
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